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The content that mixes PK-2 subsequently is until evenly.Make temperature maintenance at 50-60 ℃, through P-1 recirculation content.Initial subsequently nitrogen NF stream is opened the C-2 vacuum pump.It should be noted that and preferably avoid the product foam that rises.Subsequently batch is cooled to 45-50 ℃, opens vacuum and nitrogen NF simultaneously.When product is cooled to said temperature, close C-2 (vacuum pump), remove any vacuum with nitrogen NF.Nitrogen NF stream stays open.Purify dump valve with product subsequently, collect sample or packing product then